The
preparation called a Kermes is a metallic extract obtained from
any ore through a lye menstruum, that is by caustic soda or
Sodium Hydroxide, NaOH, in a saturated solution. According to
Fulcanelli the Kermes is "that which dyes red". In
fact the Kermes is a red coloured sediment when extracted from
Antimony by means of a lye. Some consider that the term Kermes
should be used for a specific production within the metallc
realm and not used as a general term as I have here.
This method of extracting a tincture from a metallic ore is said
to have been very popular during the renaissance period in
Europe. The example we give here is a Kermes extracted from
Antimony tri-sulphide, Sb2S3, in the form of a greyish-black
powder. This preparation (Kermes), in particular, because the
Antimony used is a sulphide and has not previously been calcined
to a white salt, or oxide, contains an extract of native or
crude sulphur. Because of this we point out that when taking, as
a medicinal preparation, the Kermes of Antimony tri-sulphide
remember that the sulphur extract will preserve any sickness
which the subject at the time might be experiencing.
Therefore, it is proper that this preparation should only be
administered to a subject when in good health in order to
preserve that condition.
(Caution: is a dangerous to experiment
with in internal consumption of alchemically prepared metallic
oils. Antimony is a dangerous poison of the same magnitude as
arsenic. We provide these instructions here simply as a method
of demonstrating the alchemical process of extracting
philosophic Sulphur (or metallic oils) and not as a guideline
for preparing alchemical medicines. Do not touch antimony with
your bare skin. Do not breath in antimony dust/powder. To do so
could be fatal.)
METHOD
EQUIPMENT:
-
150gms
Antimony tri-sulphate, Sb2S4.
-
850gms
of Caustic soda, NaOH.
-
10
litres of distilled, living, rain water.
-
2
litres Glacial Acetic acid, .
-
500mls
90% rectified Alcohol
-
Soxhlet
extractor
-
6x
1litre glass jars.
-
1
plastic bucket.
-
Rubber
gloves.
-
Face
mask.
CAUTION:
Always wear gloves when handling Antimony, Acid and Alkali.
Also, always wear a mask and work in a well ventilated
environment when working with Antimony powder, Acid and Alkali
fumes.
METHOD:
Step(1) Add 850gms of Caustic Soda to 1200mls of distilled rain
water till saturated. (Note: reaction causes heat).
Step(2) Add to this 'lye', 150gms of Antimony tri-sulphate.
Leave to cool, or cool by hand. (Note: The Caustic solution
(menstruum) should quickly extract a green tincture from the
Antimony. (This tincture originates primarily from the
combustible external, crude or native sulphur which is present
as the tri-sulphide attached to the Antimony). Some have called
this the 'Green Lion'.
Step(3) Mix 1 litre of rain water and 1 litre of Glacial Acetic
acid, into a solution. Carefully.
Step(4) Filter (fast filter), the Antimony-lye solution.
Step(5) Put filtrate into a large container (e.g. a plastic
bucket), and slowly, with care, add the Glacial-Acetic-water
solution until Ph shows neutral (7), to slightly acid.
(Note: By this action the Acetic acid neutralizes the Caustic
alkali causing a throthy brownish-red powder to appear. This is
the Kermes. At the same time the observer will notice the
pungent odour of Hydrogen Sulphide gas being released.)
Step(6) Add a good quantity of rain water to the neutral
solution containing the Kermes, and leave till the Kermes
precipitates fully.
(Note: Adding the water helps to neutralize the solution and to
wash the acid, and any residue caustic, out of the Kermes.)
Step(7) Once the Kermes has fully precipitated, pour off the
water carefully. Put the Kermes into a large filter and cover
with fresh water again to assure that any remaining acid or
alkali residue is fully washed out. If the water that passes
through the filter has a tincture, repeat, adding fresh water
until the filtrate is clear and neutral Ph.
(Note: This process is important to ensure that no caustic salts
end up in our final preparation. If, during this washing you
find that the Ph is increasingly acid stop. This is a sign that
you are beginning to wash the spirit out of the Kermes, which
will eventually lead to the impotence and death of our
preparation.)
Step(8) Dry out our Kermes slowly and carefully under an
overhead heat source.
Step(9) Grind the brown-red salt obtained from this drying to a
fine powder.
Step(10) Set up a soxhlet extractor with a sufficient amount of
either, (a) pure Glacial Acetic, or (b) a solution of half
distilled rain water and half Glacial Acetic, in the boiling
flask. Put our powdered Kermes into the sock and leave to fully
extract.
Step(11) When extraction is finished remove tincture from
boiling flask. Decant the fluid into an airtight storage jar.
Clean out any crystalline matter from boiling flask and store in
a separate jar. (Note: the product we have at this stage is
Antimony acetate, partly fluid in the form of a tincture and,
often, partly crystaline. From this point we only discuss the
further preparation of the fluid extract tincture, not the
crystaline mass. Never-the-less this mass is largely Antimony
Acetate, as we have said, and can be further prepared.)
Step(12) Filter (fine filter), the tincture, which should be a
clear red-brown, like good claret, when finished.
Step(13) Put this clear tincture into an evaporating dish and
evaporate off the acid (or acid water solution), which will
leave behind a salt of creamy-white-yellow to orange color.
Assure that this salt is completely dry. Wash carefully with
fresh water to remove all acetic but be careful that you do not
begin to wash out the spirit, which, if happening, will be
indicated by a sudden rise in acid Ph. Finally store away from
moisture in an airtight jar.
(Note: It is from this salt that our volitile red oil of
Antimony will be extracted.)
Step(14) Grind the yellow-orange salt into a fine powder.
Step(15) Set up the soxhlet again. This time place sufficient
completely rectified alcohol into the boiling flask. Set to
extract our yellow-orange powder.
Step(16) When this extraction is complete filter the tincture
obtained through a fine filter paper. The clear golden
yellow-orange to red tincture is the Balm, oil or red volitile
Sulphur of Antimony tri-sulphide.
Step(17) It is a good idea to distil off the alcohol from the
Kermes by which you will obtain the pale salt again. At this
point, when the salt is quite dry, put the absolute alcohol onto
the salt again gently turning it in your hand. Once a good
tincture has been obtained decant the volitile red oil of
Antimony-trisulphide and store the remaining salts which may
still have impurities.
Dosage:
Homeopathic dilution 1/1000 in pure spirit of wine.
Fulcanellis "The Mystery of the Cathedrals'. Quote:
"The Oak not only provides the gall, but it also gives the
kirmis (Fr. kermes), which, in the Gay Science, has the same
signification as Hermes, the initial consonants being
interchangeable. The two terms have an identical meaning, namely
Mercury. At any rate, while the gall gives the name of the raw
mercurial matter, kirmis (Arab girmiz that which dyes scarlet)
characterizes the prepared substance." And further
..."Try to separate the pure part of it, or its metallic
soul as the sacred expression has it, and you will have the
kirmis, the Hermes, the mercury dye which has within it the
mystic gold, just as St.Christopher carries Jesus and the ram
carries its own fleece."... enough said.
Native or mineral sulphur when prepared alchemically is a
preservative. Therefore any sulphide preparation, as with the
one we discuss here, should be considered a combination of the
primary metal and sulphur.
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