for information purposes only
NITRIC ACID
There
are several ways to make this most essential of all acids for explosives. One method by which it could be
made will be presented. Once again, be reminded
that these methods SHOULD NOT BE CARRIED OUT!!
Materials: sodium
nitrate or potassium
nitrate distilled
water concentrated
sulfuric acid |
Equipment: adjustable
heat source retort ice
bath stirring
rod collecting
flask with stopper |
1) Pour
32 milliliters of concentrated sulfuric acid into the retort.
2)
Carefully weigh out 58 grams of sodium nitrate, or 68 grams of potassium
nitrate. and add this to the acid slowly. If it all does not dissolve,
carefully stir the solution with a glass rod until it does.
3)
Place the open end of the retort into the collecting flask, and place the
collecting flask in the ice bath.
4)
Begin heating the retort, using low heat. Continue heating until liquid
begins`to come out`of the end of the`retort. The liquid that forms is nitric
acid. Heat until the precipitate in the bottom of the retort is almost dry, or
until no more nitric acid is forming.
CAUTION: If the acid
is headed too strongly, the nitric acid will decompose as soon as it is formed.
This can result in the production of highly flammable and toxic gasses that may
explode. It is a good idea to set the above apparatus up, and then get away
from it.
Potassium
nitrate could also be obtained from store-bought black powder, simply by dissolving
black powder in boiling water and filtering out the sulfur and charcoal. To
obtain 68 g of potassium nitrate, it would be necessary to dissolve about 90 g
of black powder in about one litre of boiling water. Filter the dissolved
solution through filter paper in a funnel into a jar until the liquid that
pours through is clear. The charcoal and sulfur in black powder are insoluble
in water, and so when the solution of water is allowed to evaporate, potassium
nitrate will be left in the jar.
for information purposes only